Process for the recovery of solid cyanuric chloride (B)

Details Process for the recovery of solid cyanuric chloride (B) Process for the recovery of solid cyanuric chloride (B)

1979-08-15

1980-08-12

Ford, John M.

Organic compounds -- part of the class 532-570 series

Organic compounds

Four or more ring nitrogens in the bicyclo ring system

C07D25128

Patent

active

042174511

ABSTRACT:
Solid cyanuric chloride is recovered by a process of spraying in the presence of a cooling medium liquid cyanuric chloride which preferably is freed from chlorine and cyanogen chloride, the cyanuric chloride is sprayed with the aid of known spraying apparatus into a separation container optionally with a propellant, while simultaneously with the cyanuric chloride spraying a liquid cooling medium through a second spraying apparatus separate from the first spraying apparatus, withdrawing the solidified cyanuric chloride from the separatory container and drawing off the resulting now gaseous cooling medium containing cyanuric chloride from the lower portion of the separatory container.

REFERENCES:
patent: 3179662 (1965-04-01), Zinsstag et al.
patent: 3256070 (1966-06-01), Trickey
patent: 3818002 (1974-06-01), Goelz et al.
patent: 3925377 (1975-12-01), Geiger et al.
patent: 4038276 (1977-07-01), Geiger et al.
Allman, "Enzyklopadie der technischen Chemie", 3rd Ed., (1954) vol. 5, pp. 624-625.
Schellenberg, Chemie, Ing. Tech., 38th year, (1966) No. 3, pp. 342-346.

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