Process for the recovery and separation of tantalum and niobium

Chemistry of inorganic compounds – Treating mixture to obtain metal containing compound – Group vb metal

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423 62, 423 64, 423 65, 423 67, 423 68, C22B 3420, C01G 3300, C01G 3500

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active

052099105

ABSTRACT:
Improved solvent extraction recovery of tantalum and niobium oxides from an acid solution of raw materials containing such oxides wherein the charged organic solvent [e.g., MIBK] is washed out (a) with 8-16N sulfuric acid and then (b) with water or dilute HF. This avoids the use of a second mineral acid addition after digestion by HF of raw materials (and avoids problems attendant to use a second mineral acid).

REFERENCES:
patent: 2962372 (1960-11-01), Foos et al.
patent: 3117833 (1964-01-01), Pierret
patent: 3712939 (1971-03-01), Chapps et al.
patent: 3972710 (1976-08-01), Meyer
patent: 4309389 (1982-01-01), Meyer

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