Process for the purification of mixtures of...

Distillation: processes – separatory – With chemical reaction – Including step of adding catalyst or reacting material

Reexamination Certificate

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C203S071000, C203S100000, C560S347000, C560S352000, C560S359000

Reexamination Certificate

active

07118653

ABSTRACT:
Process for the purification of toluenediisocyanate from a crude distillation feed which includes toluenediisocyanate, an organic solvent and less than 2% by weight phosgene by separating the crude distillation feed in a dividing-wall distillation column into at least four product fractions P1–P4.P1is a phosgene enriched low-boiler product,P2is a solvent-enriched product,P3is a high boiler enriched bottoms andP4is a toluenediisocyanate product stream.

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