Process for the purification of dialkylphosphorochloridothioates

Chemistry of carbon compounds – Dipeptides – e.g. – aspartame – anserine – carnosine – etc.

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C07F 920

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active

042474906

ABSTRACT:
A process for purification of dialkyl phosphorochloridothioate by contacting a crude material containing oxygenated phosphorus compound impurities with an alcohol and separating the product dialkyl phosphorochloridothioate from the reaction product, for example, by distillation.

REFERENCES:
patent: 3356774 (1967-12-01), Niermann et al.
patent: 3836610 (1974-09-01), Diveley
patent: 3897523 (1975-07-01), Sorstokke
patent: 4025586 (1977-05-01), Lippman
patent: 4075992 (1978-02-01), Vopel et al.
patent: 4159289 (1979-06-01), Anderson et al.

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