Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof
Patent
1977-06-17
1978-09-12
Killos, Paul J.
Organic compounds -- part of the class 532-570 series
Organic compounds
Carboxylic acids and salts thereof
562580, C07C 5916, C07C10120
Patent
active
041137710
ABSTRACT:
It is disclosed that citric acid and salts thereof are readily produced by reacting acetone dicarboxyl ions, cyanide ions and alkali metal ions to produce an intermediate system which is subsequently reacted in an excess caustic system to form a salt of citric acid and that the salt is readily recovered by precipitation from the excess caustic system under proper conditions of concentration and temperature without requiring the formation of calcium salts. The recovered salt may be used directly or may be subjected to additional purification or may be converted to citric acid or other salts thereof by treatment with an acidification system such as sulfuric acid.
REFERENCES:
patent: 3769337 (1973-10-01), Wiegand
patent: 3769338 (1973-10-01), Daganl et al.
patent: 3917685 (1975-11-01), Bergeron
Lawrence, Jr. Walter W.
McKay Tom W.
Wiegand Karl E.
Ethyl Corporation
Killos Paul J.
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