Process for the purification of a crude carboxylic acid slurry

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C562S416000, C562S485000

Reexamination Certificate

active

07132566

ABSTRACT:
Disclosed is a process to produce a purified carboxylic acid product. The process comprises removing impurities from a crude carboxylic acid slurry in a solid-liquid displacement zone to form a slurry product. The slurry product if further treated in a staged oxidation zone and a crystallization zone to from a crystallized product. The crystallized product is further cooled in a cooling zone and subsequently filtered and dried in a filtration and drying zone. The process produces purified carboxylic acid product having good color and low impurity levels without the use of purification steps like hydrogenation.

REFERENCES:
patent: 3170768 (1965-02-01), Baldwin
patent: 3584039 (1971-06-01), Meyer
patent: 3683018 (1972-08-01), Longland, Jr.
patent: 3996271 (1976-12-01), Yokota et al.
patent: 4158738 (1979-06-01), Scott et al.
patent: 4201871 (1980-05-01), Tanouchi et al.
patent: 4268690 (1981-05-01), Komatsu et al.
patent: 4314073 (1982-02-01), Crooks
patent: 4330676 (1982-05-01), Moxham
patent: 4334086 (1982-06-01), Hanotier et al.
patent: 4356319 (1982-10-01), Roffia et al.
patent: 4357475 (1982-11-01), Hanotier et al.
patent: 4447646 (1984-05-01), Johnson et al.
patent: 4588414 (1986-05-01), Takegami et al.
patent: 4605763 (1986-08-01), Kiefer et al.
patent: 4707274 (1987-11-01), Donhauser et al.
patent: 4812233 (1989-03-01), Coenen et al.
patent: 4861919 (1989-08-01), Robbins et al.
patent: 4939297 (1990-07-01), Browder et al.
patent: 5008450 (1991-04-01), Yamamoto et al.
patent: 5080721 (1992-01-01), Flanigan et al.
patent: 5095146 (1992-03-01), Zeitlin et al.
patent: 5107874 (1992-04-01), Flanigan et al.
patent: 5116423 (1992-05-01), Kokkonen et al.
patent: 5143554 (1992-09-01), Koyama et al.
patent: 5200557 (1993-04-01), Gee et al.
patent: 5359133 (1994-10-01), Nazimok et al.
patent: 5454959 (1995-10-01), Stevens
patent: 5527957 (1996-06-01), Hindmarsh et al.
patent: 5563293 (1996-10-01), Hindmarsh et al.
patent: 5583254 (1996-12-01), Turner et al.
patent: 5616792 (1997-04-01), Bartos et al.
patent: 5635074 (1997-06-01), Stenstrom et al.
patent: 5643468 (1997-07-01), Ure
patent: 5676847 (1997-10-01), Yamamoto et al.
patent: 5679846 (1997-10-01), Hindmarsh et al.
patent: 5684187 (1997-11-01), Ohkoshi et al.
patent: 5698734 (1997-12-01), Turner et al.
patent: 5712412 (1998-01-01), Inary et al.
patent: 5777161 (1998-07-01), Inary
patent: 5840965 (1998-11-01), Turner et al.
patent: 5840968 (1998-11-01), Lee et al.
patent: 5925786 (1999-07-01), Isayama et al.
patent: 5955394 (1999-09-01), Kelly
patent: 6228215 (2001-05-01), Hoffman, Jr.
patent: 6495044 (2002-12-01), Verdoes
patent: 6517733 (2003-02-01), Carlson
patent: 6797073 (2004-09-01), Teruggi et al.
patent: 2003/0004372 (2003-01-01), Piras et al.
patent: 2004/0245176 (2004-12-01), Parker et al.
patent: 2004/0260052 (2004-12-01), Nagao et al.
patent: 2005/0087215 (2005-04-01), Miyahara et al.
patent: 31 28 474 (1982-06-01), None
patent: 0111784 (1986-02-01), None
patent: 983677 (1965-02-01), None
patent: 1152577 (1969-05-01), None
patent: 1260755 (1972-01-01), None
patent: 1 358 520 (1974-07-01), None
patent: 1388289 (1975-03-01), None
patent: 48-26740 (1973-09-01), None
patent: 7-149690 (1995-06-01), None
patent: 7-291896 (1995-11-01), None
patent: 9-286758 (1997-11-01), None
patent: 9-286759 (1997-11-01), None
patent: 2001-139514 (2001-05-01), None
patent: 2001-247511 (2001-09-01), None
patent: 2001-288139 (2001-10-01), None
patent: 2002-230819 (2002-08-01), None
patent: WO 93/24440 (1993-12-01), None
patent: WO 94/17892 (1994-08-01), None
patent: WO 99/31038 (1999-06-01), None
U.S. Appl. No. 10/645,737, filed Aug. 21, 2003, Sheppard et al.
U.S. Appl. No. 10/645,734, filed Aug. 21, 2003, Sheppard et al.
PCT International Search Report.
Copending U.S. Appl. No. 10/758,676 filed Jan. 15, 2004 by Parker et al.
Copending U.S. Appl. No. 10/872,248 filed Jun. 18, 2004 by Sheppard.
Copending U.S. Appl. No. 11/346,393 filed Feb. 2, 2006.
USPTO Office Action dated Nov. 30, 2004 for U.S. Appl. No. 10/645,734.
USPTO Office Action dated Apr. 21, 2004 for U.S. Appl. No. 10/645,734.
USPTO Office Action dated Apr. 22, 2003 for U.S. Appl. No. 10/315,294.
USPTO Office Action dated Dec. 10, 2004 for U.S. Appl. No. 10/645,737.
USPTO Office Action dated Apr. 19, 2004 for U.S. Appl. No. 10/645,737.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Process for the purification of a crude carboxylic acid slurry does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for the purification of a crude carboxylic acid slurry, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for the purification of a crude carboxylic acid slurry will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-3623230

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.