Process for the production of S,S,S-tributylphosphorotrithioate

Details Process for the production of S,S,S-tributylphosphorotrithioate Process for the production of S,S,S-tributylphosphorotrithioate

1994-08-30

1995-11-14

Richter, Johann

Organic compounds -- part of the class 532-570 series

Organic compounds

Phosphorus esters

558208, C07F 911

Patent

active

054668522

ABSTRACT:
S,S,S-tributylphosphorotrithioite is oxidized with a perborate or percarbonate at a pH of from about 6 to about 12 and at a temperature of from about 40.degree. to about 65.degree. C. Sodium perborate is a particularly preferred oxidizing agent. The product S,S,S-tributylphosphorotrithioate may be recovered by simple phase separation.

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L. Huestis, J. Chem. Ed., 54, 327 (1977).
D. S. Matteson & R. J. Moody, J. Org. Chem., 45, 1091 (1980).

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