Process for the production of pure tetrazole-1-acetic acid

Details Process for the production of pure tetrazole-1-acetic acid Process for the production of pure tetrazole-1-acetic acid

1974-09-27

1976-01-13

Waddell, Frederick E.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260308D, C07D25704

Patent

active

039324419

ABSTRACT:
Process for producing tetrazole-1-acetic acid of maximum purity includes the steps of providing a crude reaction product containing an alkyl ester of tetrazole-1-acetic acid having from 1 to 4 carbon atoms in the alkyl group, effecting molecular distillation of this reaction product at a temperature below 130.degree.C. under a vacuum of 10.sup.-.sup.1 torr to obtain a distillant containing the alkyl ester and then gently hydrolyzing the resultant distillate to obtain the desired acid product.

REFERENCES:
can. J. Chem. 47 (1969), pp. 813-819.

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