Organic compounds -- part of the class 532-570 series – Organic compounds – Four or more ring nitrogens in the bicyclo ring system
Patent
1977-01-27
1978-05-09
Jiles, Henry R.
Organic compounds -- part of the class 532-570 series
Organic compounds
Four or more ring nitrogens in the bicyclo ring system
544 86, 4242484, C07D29506
Patent
active
040888177
ABSTRACT:
An improvement in the process for the production of P-1487 from the reaction of 1-nitropropane, 37% formaldehyde and morpholine, the improvement comprising mixing 1-nitropropane and 37% formaldehyde at a temperature of 40.degree.-42.degree. C., adding morpholine maintaining the temperature at 40.degree.-42.degree. C., holding the mixture for two hours at 40.degree.-42.degree. C., cooling to allow layer separation, separating the upper oil layer and concentrating the oil layer to P-1487 by removing excess water.
REFERENCES:
patent: 2474791 (1949-06-01), Senkus
Hunsucker Jerry H.
Shelton Robert W.
Dewey Robert H.
IMC Chemical Group, Inc.
Jiles Henry R.
Ramsuer R. W.
Williams Roger A.
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