Process for the production of mesophase pitch

Mineral oils: processes and products – Asphalts – tars – pitches and resins; making – treating and...

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208 4, 208 6, 208 44, 4234474, 4234476, 4234477, 4234478, C10G 2700, C10C 304, C10C 302

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049043714

ABSTRACT:
An improved process for producing an anisotropic pitch product suitable for carbon fiber manufacture. A carbonaceous feedstock substantially free of mesophase pitch is heated for a period of time at an elevated temperature while passing an oxidatively reactive sparging gas such as a mixture of oxygen and nitrogen through the feedstock. The oxidatively treated feedstock is then subjected to a heat soak, for a longer period of time in the absence of a sparging gas. Thereafter the heat soaked feedstock is heated at an elevated temperature in the presence of a non-oxidative sparging gas for a time period equal to or less than the heat soak to produce an anisotropic pitch having from 50 to 100% by volume mesophase which is suitable for producing good quality carbon fibers.

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