Process for the production of linear condensates of phenol and f

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From phenol – phenol ether – or inorganic phenolate

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264176F, 528140, 528129, C08G 810

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active

041196112

ABSTRACT:
A two-stage process for making a linear condensate of phenol and formaldehyde which can be extruded as a film or thread. In the first stage phenol and formaldehyde are reacted at about 90.degree. C to produce a clear low-viscosity phenol-methylol liquid, the pH of which is adjusted to a value greater than 3, say between 3.5 and 7. In the second stage the product of the first stage is added in aliquot portions to molten phenol having a pH of 3 or less, while maintaining the temperature at about 100.degree. C. After all the phenol-methylol has been added the mixture is slowly heated as the viscosity increases up to about 150.degree. C until there is no further increase in viscosity. The highly viscous end product can be extruded as a film or thread.

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patent: 3876620 (1975-04-01), Moss
patent: 3959433 (1976-05-01), Sauers

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