Process for the production of improved polyaminopolyamide epichl

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Mixing of two or more solid polymers; mixing of solid...

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525435, C08G 6948

Patent

active

051717956

ABSTRACT:
A process for the manufacture of improved water soluble polyaminopolyamide-epichlorohydrin resins is disclosed. The polyaminopolyamide-epichlorohydrin reaction is continued until between 70% to 100% of the total charge of epichlorohydrin has reacted. The polyaminopolyamide-epichlorohydrin mixture is then treated with a specified amount of a halogen-free mineral acid. Preferably the mineral acid is selected from the group consisting of sulphuric acid, phosphoric acid, nitric acid and sodium hydrogen sulphate. Following the completion of the acid addition the reaction is continued to effect at least a 10% reduction in the polymer bound organochlorine concentration, based on the composition of the reaction mixture at the time of the acid addition.

REFERENCES:
patent: 2926116 (1960-02-01), Keim
patent: 3197427 (1965-07-01), Schmaltz
patent: 3891589 (1975-06-01), Ray-Chauduri
patent: 4857586 (1989-08-01), Bachem et al.

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