Chemistry of inorganic compounds – Halogen or compound thereof – Binary compound containing metal
Patent
1977-03-29
1978-02-21
Stern, Edward
Chemistry of inorganic compounds
Halogen or compound thereof
Binary compound containing metal
423499, 423554, C01F 530, C01F 500, C01D 306, C01F 540
Patent
active
040753093
ABSTRACT:
Concentrated magnesium chloride solutions are prepared from industrial liquors or brines by evaporating the liquor in a vacuum in two or more stages in a counter current evaporator with crystallization characteristics up to a final concentration of 440 to 475 g/l MgCl.sub.2, a solid content of 12 to 25% by weight and a final temperature of 95.degree. to 105.degree. C, whereafter the liquor is separated from crude crystallized carnallite and sodium chloride, is debrominated by the addition of chlorine, is neutralized by the addition of lime or dolomite milk, is separated in the heat from solid substances, is cooled to effect further crystallization, and is finally separated as a concentrated magnesium chloride solution containing 400 to 465 g/l MgCl.sub.2.
REFERENCES:
patent: 1012387 (1911-12-01), Malcolm et al.
patent: 2479001 (1949-08-01), Burke et al.
patent: 3729550 (1973-04-01), Boyum et al.
Kirchner Siegfried
Kunze Dietmar
DeLaurentis Anthony J.
Kali und Salz Aktiengesellschaft
Stern Edward
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