Process for the production of glycine enriched NaCI crystals...

Drug – bio-affecting and body treating compositions – Inorganic active ingredient containing – Alkali or alkaline earth chloride

Reexamination Certificate

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C424S489000, C514S561000, C426S649000, C426S806000

Reexamination Certificate

active

10745758

ABSTRACT:
The present invention relates to a simple, economical, and efficient cyclic process for producing rhombic dodecahedron shaped glycine enriched, free flowing common salt from brine, said process comprising steps of adding glycine of concentration ranging between 10 to 25% to the saturated brine, evaporating the saturated brine containing glycine to obtain crystals having high content of glycine, with mother liquor, washing the crystals with saturated brine to obtain rhombic dodecahedron shaped glycine enriched common salt having glycine content ranging between 0.5 to 1.0% and a washed brine, combining the mother liquor and the washed brine to obtain resulting brine, subjecting the resultant brine to solar evaporation, and repeating the steps of (iii) to (v) to obtain rhombic dodecahedron shaped glycine enriched common salt from brine with glycine concentration ranging between 0.5 to 1.0%.

REFERENCES:
patent: 3985801 (1976-10-01), Thunberg et al.
Fenimore, C.P. et al., “The mutual habit modification of sodium chloride and dipolar ions,” Journal of the American Chemical Society, vol. 71, pp. 2714-2717 (1949).

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