Process for the production of fatty acid amides

Organic compounds -- part of the class 532-570 series – Organic compounds – Fatty compounds having an acid moiety which contains the...

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C554S068000

Reexamination Certificate

active

07098351

ABSTRACT:
This invention discloses a rapid method of production for fatty acid amide from fatty acid and urea. One example is the preparation of oleylamide from oleic acid and urea. The yields are high and oleylamide is selectively formed by judicious choice of catalyst. The production of fatty acid amide involves heating fatty acid and urea in a microwave oven with the use of Lewis acid catalyst. The product from the reaction is subjected to solvent extraction with chloroform and then followed by purification with n-hexane, ethanol and acetonitrile via recrystalization method. Such an oleylamide is preferred for application as a mould release agent, slip agent in plastic film production, water repellent and as a raw material for cosmetics production.

REFERENCES:
patent: 2013108 (1935-09-01), Reppe et al.
patent: 2070991 (1937-02-01), Hund et al.
patent: 3253006 (1966-05-01), Davis et al.
patent: 3816483 (1974-06-01), Werdehausen et al.
patent: 4277410 (1981-07-01), Li et al.
patent: 4655972 (1987-04-01), Eikelboom et al.
Beckwith, “Synthesis of Amides”.
National Dairy Products Corporation, “Manufacture of Amide Compounds”, GB 939378, (Oct. 16, 1963).
Cravatt, et al., Structure Determination of an Endogenous Sleep-Inducing Lipid,cis-9-Octadecenamide (Oleamide): A Synthetic Approach to the Chemical Analysis of Trace Quantities of Natural Product, 1996 American Chemical Society, pp. 580-590, Sep. 21, 1995.
Jasperse, “The Determination of Fatty Amides by High Performance Liquid Chromatography”, JAOCS, vol. 65, No. 11, pp. 1804-1807, (Nov. 1988).

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Process for the production of fatty acid amides does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for the production of fatty acid amides, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for the production of fatty acid amides will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-3682357

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.