Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing
Patent
1985-03-12
1987-05-05
Miller, Edward A.
Organic compounds -- part of the class 532-570 series
Organic compounds
Oxygen containing
568939, C07C 7910
Patent
active
046634908
ABSTRACT:
In the production of dinitrotoluene by a two-stage reaction of toluene with nitric acid in the presence of sulphuric acid, wherein toluene is nitrated to mononitrotoluene in the first stage using spent acid from the second stage, and the mononitrotoluene is nitrated to dinitrotoluene in the second stage using concentrated spent acid from the first stage, the improvement which comprises concentrating spent acid under vacuum in an indirectly-heated evaporator and feeding mononitrotoluene into the superheated vapor of the evaporator.
REFERENCES:
patent: 2256999 (1941-09-01), Castner
patent: 3178481 (1965-04-01), Hauze
patent: 4091042 (1978-05-01), Alexanderson et al.
patent: 4274910 (1981-06-01), Forter et al.
patent: 4367347 (1983-01-01), Sawicki
patent: 4496782 (1985-01-01), Carr
patent: 4600702 (1986-07-01), Schumacher
Becher Dieter
Gerken Rudolf
Lailach Gunter
Witt Harro
Bayer Aktiengesellschaft
Miller Edward A.
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