Organic compounds -- part of the class 532-570 series – Organic compounds – Nitriles
Patent
1985-01-10
1988-07-05
Brust, Joseph Paul
Organic compounds -- part of the class 532-570 series
Organic compounds
Nitriles
512 6, C07C12000, C07C12148
Patent
active
047556153
ABSTRACT:
Cyclododecenylacetonitrile is prepared by reacting cyclododecanone with cyanoacetic acid in the presence of a catalyst. Purified cyclododecenylacetonitrile has a pleasant scent reminiscent of roses and lilies of the valley, containing additionally a musk note, and is suitable as a fragrance and as a fragrance component.
REFERENCES:
House, "Modern Synthetic Reactions", pp. 649-650, 2nd. ed., (1972); W. A. Benjamin Inc. Menlo Park, Calif., Reading, Mass., London, Amsterdam, Sydney.
Di Biase, et al.; J. of Org. Chem. (1979), 44, p. 4640.
House, "Modern Synthetic Reactions", p. 646, (1972), 2nd ed., W. A. Benjamin, Inc., Menlo Park, Calif., Reading, Mass.
Chemical Abstracts vol. 71, No. 3, (Jul. 21, 1969), p. 280, No. 12673S, Nobou Itoh et al.
R. Adams, et al, "Organic Reactions", vol. 15, (1967), pp. 204, 236-238.
Helvetica Chimica Acta, vol. 53, Section 6, No. 186-186, (Oct. 16, 1950) pp. 1437-1448, O. Schnider et al.
Synthesis, International Journal of Methods in Synthetic Organic Chemistry, No. 9, (Sep. 1977), pp. 629-632, Di Biase et al.
Helvetica Chimica Acta, vol. 62, Section 3, No. 92, (Apr. 20, 1979), pp. 882-893, A. Fischli.
De Biase et al, J. Org. Chem., vol. 44, No. 25, (1979), "Direct Synthesis of, -Unsatured Nitriles . . . etc.", pp. 4640-4649.
G. Jones, Organic Reactions, vol. 15, pp. 204-207, (1967), "The Knoevenagel Condensation".
Organikum, Organisch-Chemisches Grundpraktikum, 13.Auflage, pp. 508-509, 571, (1974).
Andre Slagmulder
Kaufhold Manfred
Brust Joseph Paul
Huels Aktiengesellschaft
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