Process for the production of benzothiazole sulphene amides

Organic compounds -- part of the class 532-570 series – Organic compounds – Four or more ring nitrogens in the bicyclo ring system

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544368, 546198, 548167, 548168, C07D27780, C07D41312

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active

048017078

ABSTRACT:
Benzothiazole sulphene amides are obtained from dibenzothiazolyl disulphide and water-soluble amines in the absence of an oxidizing agent and in the presence of aqueous alkali in a high yield and with very good stability in storage by placing the amine solution in water and simultaneously adding dibenzothiazolyl disulphide and aqueous alkali from separate storage vessels.

REFERENCES:
patent: 4127454 (1978-12-01), Torii et al.
patent: 4182873 (1980-01-01), Janin
Isv. Vyssh. Uchebn. Zaved., Khimiya i khim. tekhnol., 22 (1979), 9, 1067-1070.

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