Process for the production of 5-benzyl-3-furfuryl alcohol

Details Process for the production of 5-benzyl-3-furfuryl alcohol Process for the production of 5-benzyl-3-furfuryl alcohol

2006-03-28

2006-03-28

Saeed, Kamal A. (Department: 1626)

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

Reexamination Certificate

active

07019154

ABSTRACT:
Synthesis process of 5-benzyl-3-furfuryl alcohol including the reduction reaction with NaBH4or with sodium dihydro bis-(2-methoxyethoxy)aluminium hydride of 3-benzyl-5-hydroxymethyl-5-carboxyalkyl isoxazoline to give 3-benzyl-5,5-bis(hydroxymethyl)isoxazoline which, through subsequent reduction in the presence of a weak protic acid and consequent rearrangement with strong aqueous acid, gives 5-benzyl-3-furfuryl alcohol.

REFERENCES:
Database Crossfire Beilstein 'Online!, Beilstein Institut zur Förderung der Chemischen Wissenschaften, Frankfurt am Main, DE; Database accession No. 139508, XP002213661, Abstract, & Mnoshojan, Afrikjan: Dokl. Akad. Nauk. Arm. Ssr. vol. 25, 1957, p. 201.
Mimi L. Quan et al., “Design and Synthesis of Isoxazoline Derivatives as Factor Xa Inhibitors,” J. Med. Chem., vol. 42, No. 15 1999, pp. 2760-2773, XP002213660.

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