Organic compounds -- part of the class 532-570 series – Organic compounds – Four or more ring nitrogens in the bicyclo ring system
Patent
1978-07-17
1979-02-20
Trousof, Natalie
Organic compounds -- part of the class 532-570 series
Organic compounds
Four or more ring nitrogens in the bicyclo ring system
C07D29506
Patent
active
041408551
ABSTRACT:
In a process for the production of 2-nitrobutylmorpholine from 1-nitropropane, morpholine and formaldehyde the improvement comprising mixing 1-nitropropane and morpholine, heating to about 55-60.degree. C., adding formaldehyde over about a 3-4 hour period, holding the reaction mixture at about 55-60.degree. C. for about a 2-3 hour period to make a total addition/holding period of at least six hours, cooling the reacton mixture to form a two phase oil/aqueous system and concentrating the oil layer to 2-nitrobutylmorpholine by removing excess water and 1-nitropropane.
Dewey Robert H.
International Minerals & Chemical Corp.
Post Howard E.
Ramsuer R. W.
Trousof Natalie
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