Process for the production of 2-aryl-2H-benzotriazoles

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07D24920

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041419030

ABSTRACT:
A process for the production of 2-aryl-2H-benzotriazoles comprises reducing and cyclizing the corresponding o-nitroazobenzenes with carbon monoxide at a temperature in the range of about 20.degree. C. to about 150.degree. C. and at a pressure in the range of about 15 psia (1 atmosphere) to about 1000 psia (66 atmospheres) in an alkaline medium at a pH over 10 in the presence of a copper-amine complex catalyst. High yields of pure product are obtained with a concomitant reduction of undesired by-products and a reduction in effluent pollution problems.

REFERENCES:
patent: 3978074 (1976-08-01), Jancis

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