Process for the production of 1-n-dodecylazacycloheptan-2-one

Details Process for the production of 1-n-dodecylazacycloheptan-2-one Process for the production of 1-n-dodecylazacycloheptan-2-one

1989-12-15

1990-11-27

Bond, Robert T.

Organic compounds -- part of the class 532-570 series

Organic compounds

Unsubstituted hydrocarbyl chain between the ring and the -c-...

540485, C07D22310

Patent

active

049736884

ABSTRACT:
There is disclosed a method for the production of 1-n-dodecylazacycloheptan-2-one by reacting caprolactam with 1-bromododecane in the presence of a phase transfer catalyst under anhydrous conditions using a nonpoisonous hydrocarbon as solvent. The method is a one-pot synthesis employing solid-liquid phase transfer catalysis.

REFERENCES:
patent: 4422970 (1983-12-01), Radadhyarsa et al.
patent: 4692523 (1987-09-01), Schorr et al.

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