Process for the producing .epsilon.-caprolactam from the distill

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07D20104

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041418964

ABSTRACT:
A process for the production of .epsilon.-caprolactum from cyclohexanone oxime by rearrangement in the gaseous phase on a fluid-bed catalyst containing boron oxide, wherein residues from the distillation of cyclohexanone oxime are introduced into the reaction in liquid form, and wherein from 5 to 500 times their quantity of cyclohexanone oxime in vapor form and at least 50 times their quantity of inert gas are present during the reaction.

REFERENCES:
patent: 3210338 (1965-10-01), Huber et al.
patent: 3586668 (1977-06-01), Immel et al.
patent: 3592809 (1971-07-01), Immel et al.

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