Process for the preparation of very highly alkaline, calcium-bas

Compositions – Electrolytes for electrical devices

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252 33, 252 334, 252 39, 252 407, 252 427, 252 18, G10M12900, G10M13500

Patent

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046981705

ABSTRACT:
Disclosed is a process for preparing very highly alkaline, calcium-based, detergent-dispersant additives for lubricating oils and products produced by such a process. The process includes the steps of reacting an alkylbenzenesulfonic acid, an alkylphenol, diluent oil, halogen ions and lime, removing water formed during the reaction, sulfurizing the resultant product in the presence of glycol and at least one additional alcohol having a boiling point in excess of about 155.degree. C., carbonating the sulfurized product, removing the glycol and heavy alcohol from the sulfurized, carbonated reaction product, and filtering to remove sediment and to obtain a reaction product comprising a highly-alkaline, calcium-based detergent-dispersant additive for lubricating oils.

REFERENCES:
patent: 3178368 (1965-04-01), Hanneman
patent: 3256186 (1966-06-01), Greenwald
patent: 3350308 (1967-10-01), McMillen
patent: 3365396 (1968-01-01), Schlicht
patent: 3493516 (1970-02-01), Allphin et al.
patent: 3544463 (1970-12-01), Koft, Jr.
patent: 4057504 (1977-11-01), Shiga et al.
patent: 4251379 (1981-02-01), Le Coent et al.

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