Process for the preparation of traumatin

Details Process for the preparation of traumatin Process for the preparation of traumatin

1980-10-03

1981-09-22

Niebling, John F.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260406, C11C 100

Patent

active

042909660

ABSTRACT:
Traumatin, 12-oxo-trans (E) -10-docecenoic acid, is prepared from 10-oxomethyldecanoate by reaction with (triphenylphosphoranylene)acetaldehyde to form 12-oxomethyldodecenoate; blocking the 12-oxo group; hydrolyzing the ester group; and deblocking the 12-oxo group.

REFERENCES:
Kajiwara et al., Agric. Biol. Chem., 41 (9) pp. 1793-1794 (1977).
Bestmann et al., Tet. Lett., 1, pp. 121-124 (1977).
Yamamoto et al., Chem. Lett., pp. 859-862 (1978).
Rakoff et al., Synthetic Comm., 9, pp. 185-199 (1979).

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