Process for the preparation of titanocene dichloride

Details Process for the preparation of titanocene dichloride Process for the preparation of titanocene dichloride

1999-10-28

2000-05-16

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heavy metal containing

C07F 1300

Patent

active

060639504

ABSTRACT:
The present invention is directed to a process for the preparation of titanocene dichloride (Cp.sub.2 TiCl.sub.2) from the titanocene dimer (Cp.sub.2 TiMe).sub.2 O), which is produced as a by-product from employing the reagent dimethyl titanocene (Cp.sub.2 Ti(CH.sub.3).sub.2) in the methylenation of carbonyl compounds, such as esters and lactones.

REFERENCES:
patent: 5847176 (1998-12-01), Sullivan
patent: 5892082 (1999-04-01), Cai et al.

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