Process for the preparation of titanium thio-derivatives

Details Process for the preparation of titanium thio-derivatives Process for the preparation of titanium thio-derivatives

1975-04-29

1977-08-02

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260429CY, C07F 728

Patent

active

040395669

ABSTRACT:
A thio-derivative of titanium, represented by the formulae: ##STR1## WHEREIN CP IS A CYCLOPENTADIENE AND R is an alkyl, aryl or cycloalkyl radical, is prepared by reacting a carbonyl derivative of titanium, represented by the formula: Ti cp.sub.2 (CO).sub.2, wherein cp has the meaning given above, with a disulfide represented by the formula: R.sub.2 S.sub.2, wherein R has the meaning given above, in an inert atmosphere.

REFERENCES:
patent: 3030395 (1962-04-01), Giddings
patent: 3361777 (1968-01-01), King
patent: 3644447 (1972-02-01), Joshi
Coutts et al., Aus. J. Chem. V19, 1377-1380 (1966).
Advances in Organometallic Chemistry, vol. 9, pp. 175-176, (1970).

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