Process for the preparation of thermotropic aromatic polyesters

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From phenol – phenol ether – or inorganic phenolate

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528176, 528190, 528192, 528193, C08G 6302

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active

057314012

ABSTRACT:
A new process is provided for the formation of aromatic polyesters directly from the reaction of dialkyl ester of an aromatic carboxylic acid with dihydric phenols. The polycondensation is carried out in the presence of (a) a condensing agent; (b) a catalyst selected from the group consisting of derivatives of Group I metals, derivatives of Group IV A metals, derivatives of Group IV B metals, and mixtures thereof; and (c) a co-catalyst selected from the group consisting of methanesulfonic acid, sulfuric acid, p-toluenesulfonic acid, alkanoic acid having the formula, C.sub.n H.sub.x F.sub.y COOH, where n is an integer from 1 to 4, x and y are integers from 0 to 2n+1, and the sum of x and y is 2n+1, and mixtures thereof; at suitable temperature and pressure conditions and for a sufficient period of time to form the aromatic polyester.

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Tsutomu Oishi and H. K. Hall, Jr., Model Studies and a New Melt Polycondensation Route to Poly-Bisphenol A-Iso/terephthalate (Polyarylate), Polyarylates, pp. 83-89.
G. Bier, Polyarylates (polyesters from aromatic dicarboxylic acids and bisphenols), Polymer, 1974, vol. 15, Aug., pp. 527-535.

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