Process for the preparation of the salts of...

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

Reexamination Certificate

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Reexamination Certificate

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07880016

ABSTRACT:
The invention relates to a process for preparing a salt of an optionally substituted 4-benzimidazol-2-ylmethylamino)-benzamidine, characterised in that(a) an optionally correspondingly substituted diaminobenzene is condensed with 2-[4-(1,2,4-oxadiazol-5-on-3-yl)-phenylamino]-acetic acid,b) i) the product thus obtained is hydrogenated,ii) optionally the amidino group is carbonylated, without isolating the intermediate product of the hydrogenation beforehand andiii) without prior isolation of the intermediate product of the carbonylation the desired salt is isolated.

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Anbazhangan, et al., “Direct conversion of amidoximes to amidines via transfer hydrogenation,” 2003, p. 2467-2469, No. 16, Synthesis, Department of Chemistry, Georgia State University, Atlanta, GA, USA.
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