Process for the preparation of the boron difluoride chelate...

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

Reexamination Certificate

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C546S090000

Reexamination Certificate

active

07365201

ABSTRACT:
A process for the preparation of the boron difluoride chelate of 1-cyclopropyl-6,7-difluoro-1,4-dihydro-8-methoxy-4-oxo-3-quinolone carboxylic acid via:(a) the reaction of 1-cyclopropyl-6,7-difluoro-1,4-dihydro-8-methoxy-4-oxo-3-quinolone carboxylic acid ethyl ester with,(b) fluoroboric acid in the presence of poly(methylhydrosiloxane) or hexamethyldisiloxane.

REFERENCES:
patent: 4940794 (1990-07-01), Hermecz et al.
patent: 4980470 (1990-12-01), Masuzawa et al.
patent: WO 2004/101527 (2004-11-01), None
patent: WO 2005/047260 (2005-05-01), None

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