Process for the preparation of tetrabromobisphenol-A

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

568722, 568723, 568727, 568779, 568776, 568726, C07C 3768

Patent

active

060841362

ABSTRACT:
This invention relates to a process for the production of tetrabromobisphenol-A by the bromination of bisphenol-A, which process features: (a) feeding to a reaction mass (i) bisphenol-A and (ii) a stream of gaseous bromine, the gaseous stream having a Reynold's No. .gtoreq.40,000; (b) the reaction mass containing from about 50 to about 20,000 ppm unreacted bromine and less than 20 wt % HBr; and (c) the reaction mass having precipitated therefrom tetrabromobisphenol-A, all of (a)(ii), (b) and (c) occurring during the bisphenol-A feed.

REFERENCES:
patent: 2455652 (1948-12-01), Bralley et al.
patent: 3029291 (1962-04-01), Dietzler
patent: 3143575 (1964-08-01), Bryner et al.
patent: 3182088 (1965-05-01), Hennis
patent: 3234289 (1966-02-01), Hennis
patent: 3363007 (1968-01-01), Majewski et al.
patent: 3546302 (1970-12-01), Asadorian et al.
patent: 3868423 (1975-02-01), Montanari et al.
patent: 3929907 (1975-12-01), Janzon et al.
patent: 4013728 (1977-03-01), Brackenridge
patent: 4036894 (1977-07-01), Jenkner
patent: 4112242 (1978-09-01), Swietoslawski et al.
patent: 4180684 (1979-12-01), Kleinschmit et al.
patent: 4282391 (1981-08-01), Quinn et al.
patent: 4283566 (1981-08-01), Mark
patent: 4291177 (1981-09-01), Mark et al.
patent: 4302614 (1981-11-01), Dannenberg et al.
patent: 4451675 (1984-05-01), Bounds
patent: 4628124 (1986-12-01), McKinnie et al.
patent: 4692555 (1987-09-01), Shin
patent: 4701568 (1987-10-01), McKinnie et al.
patent: 4783556 (1988-11-01), Mitchell et al.
patent: 4909997 (1990-03-01), Mitchell et al.
patent: 4990321 (1991-02-01), Sato et al.
patent: 5008469 (1991-04-01), Eguchi et al.
patent: 5017728 (1991-05-01), McKinnie et al.
patent: 5059722 (1991-10-01), Mitchell et al.
patent: 5059726 (1991-10-01), Eguchi et al.
patent: 5068463 (1991-11-01), Walter
patent: 5107035 (1992-04-01), Hines et al.
patent: 5138103 (1992-08-01), Eguchi et al.
patent: 5208389 (1993-05-01), McKinnie et al.
patent: 5237112 (1993-08-01), LaRose
patent: 5283375 (1994-02-01), McKinnie et al.
patent: 5302761 (1994-04-01), Tamabayashi et al.
patent: 5446212 (1995-08-01), Sanders et al.
patent: 5527971 (1996-06-01), McKinnie
patent: 5723690 (1998-03-01), McKinnie
patent: 5847232 (1998-12-01), McKinnie
Chemical Abstract No. 78(1):3946j--Chemical Abstracts, vol. 78, 1973, p. 328.
Chemical Abstract No. 86(25):189500c--Chemical Abstracts, vol. 86, 1977, p. 570.
Chemical Abstract No. 96(19):162322r--Chemical Abstracts, vol. 96, 1982, p. 718.
Chemical Abstract No. 104(17):148492y--Chemical Abstracts, vol. 104, 1986, p. 656.
Chemical Abstract No. 104(23):206899z--Chemical Abstracts, vol. 104, 1986, p. 716.
Islam et al., "Tetrahalogenated 4:4'-Dihydroxydiphen;ylalkanes, their Synthesis and some of their Reactions," Egypt. J. Chem. 20, No. 5, pp. 483-490 (1977).
Sadygov, et al., "Oxidative bromination of 2,2-bis(4'-hydroxyphenyl)propane," Institute of Organochlorine Synthesis, Academy of Sciences of the Azerbaidzhan SSR, Sumgait, U.S.S.R., 1990, pp. 109-112 (Translation attached--pp. 1-7).
Levenspiel, Chemical Reaction Eng., (1962), p. 126.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Process for the preparation of tetrabromobisphenol-A does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for the preparation of tetrabromobisphenol-A, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for the preparation of tetrabromobisphenol-A will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-1487985

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.