Process for the preparation of sulfhydryl containing tricyclic l

Details Process for the preparation of sulfhydryl containing tricyclic l Process for the preparation of sulfhydryl containing tricyclic l

1990-02-09

1992-03-10

Lee, Mary C.

Organic compounds -- part of the class 532-570 series

Organic compounds

Unsubstituted hydrocarbyl chain between the ring and the -c-...

540522, C07D22314

Patent

active

050951106

ABSTRACT:
This invention relates to a process for preparing an olifinated tricyclic lactam which comprises reacting an amine with alkylnitrite to form a diazoamide compound which is further reacted with strong acid and phosphine, and finally with a strong base and formaldehyde.

REFERENCES:
Noller, Textbook of Organic Chemistry, 3rd ed., W. B. Saunders Co., Philadelphia, 1966, p. 430.
McPhee, W. D. et al., Organic Syntheses Collective, vol. 3, 119-120 (1955).
Isler, O. et al., Helvetica Chimica Acta., 40 No. 139, 1242-1249 (1957).
Wiley, P. F. et al., J. Org. Chem., 41, No. 10, 1858-1862, (1976).

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