Process for the preparation of secondary alkyl sulfate-containin

Details Process for the preparation of secondary alkyl sulfate-containin Process for the preparation of secondary alkyl sulfate-containin

1992-09-28

1993-10-05

Cintins, Marianne M.

Organic compounds -- part of the class 532-570 series

Organic compounds

Sulfate esters

558 42, C07C31504

Patent

active

052507181

ABSTRACT:
This invention relates to a process for preparing secondary alkyl sulfate-containing surface active compositions substantially free of unreacted organic matter and water, which process comprises: a) sulfating a reactant selected from the group consisting of a detergent range olefin having from about 8 to about 22 carbon atoms, a detergent range alcohol having from about 8 to about 22 carbon atoms and mixtures thereof, with a sulfating agent, b) neutralizing the product of step a) with a base dispersed in a non-surfactant carrier, c) saponifying the product of step b) , d) passing the product of step c) through a thin film evaporator to evaporate unreacted organic matter from said product and recovering a secondary alkyl sulfate-containing product.

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Asinger, "The Hydration of Olefins to Alcohols," Mono-olefins: Chemistry and Technology, 1968, pp. 689-704.

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