Process for the preparation of phosphorus pentachloride

Chemistry of inorganic compounds – Phosphorus or compound thereof – Halogen containing

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C01B 2510

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active

039950131

ABSTRACT:
Processes for the preparation of high-purity free-flowing crystalline powder phosphorus pentachloride which processes comprise reacting phosphorus trichloride with a deficit of chlorine, cooling the reaction mixture to form a crystalline mass containing the pentachloride, and recovering and/or purifying the pentachloride.

REFERENCES:
patent: 1888713 (1932-11-01), Britton et al.
patent: 1906440 (1933-05-02), Wirth

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