Process for the preparation of perylene-3,4,9,10-tetracarboxylic

Compositions: coating or plastic – Materials or ingredients – Pigment – filler – or aggregate compositions – e.g. – stone,...

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546 37, C09B 6720, C07D47106

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active

047971622

ABSTRACT:
A process for the preparation of perylene-3,4,9,10-tetracarboxylic acid N,N'-dimethylimide in a high-hiding pigmentary form and a pure red shade, in which a finely divided, dry perylene-3,4,9,10-tetracarboxylic acid, N,N'-dimethylimide prepigment which is prepared in a conventional manner and has a crystallite size of <400 .ANG. is treated with an organic solvent which is liquid in the treatment temperature range stated below and is selected from the series comprising saturated aliphatic brominated or chlorinated hydrocarbons, aromatic hydrocarbons and aromatic brominated or chlorinated hydrocarbons, in a mill or a disperser at temperatures from 0.degree. C. to 100.degree. C., the organic solvent is then distilled off and the perylene-3,4,9,10-tetracarboxylic acid N,N'-dimethylimide pigment is isolated.

REFERENCES:
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patent: 3976649 (1976-08-01), Fabian et al.
patent: 4018791 (1977-04-01), Spietschka et al.
patent: 4189582 (1980-02-01), Hoch et al.
patent: 4496731 (1985-01-01), Spietschka et al.
Herbst, Willy: Industrielle Organische Pigmente: Herstellung, Eigenschaften, Anwendung/Willy Herbst; Klaus Hunger-Weinheim: VCH, 1987.

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