Process for the preparation of octa-2,7-dienyl-1-amine from buta

Details Process for the preparation of octa-2,7-dienyl-1-amine from buta Process for the preparation of octa-2,7-dienyl-1-amine from buta

1999-02-25

2000-04-18

Barts, Samuel

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

C07C20904

Patent

active

060517387

ABSTRACT:
Process for the preparation of octa-2,7-dienyl-1-amine by telomerization of butadiene with ammonia in a two-phase system in the presence of hydrophilic palladium complexes, characterized in that octa-2,7-dienyl-1-amine and octa-1,7-dienyl-3-amine are isolated separately from one another from the reaction mixture present after telomerization, and the octa-1,7-dienyl-3-amine isolated in this way is subjected to an isomerization reaction to form octa-2,7-dienyl-1-amine, and also novel triphenylphosphine mono- and dimethoxytri(sodium sulphonates) and the use of triphenylphosphine trimethoxytri(sodium sulphonates), triphenylphosphine trimethyltri(sodium sulphonates) and triphenylphosphine trifluorodi- and tri(sodium sulphonates) as ligands for the preparation of palladium complexes.

REFERENCES:
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patent: 5756846 (1998-05-01), Driessen-Holscher et al.
patent: 5834611 (1998-11-01), Driessen-Holscher et al.
Agnew, Chemie, 107, 893 (month unavailable) 1995.
J. Prakt Chem. 335, 591 (month unavailable) 1994.

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