Process for the preparation of norpatchoulenol and intermediates

Details Process for the preparation of norpatchoulenol and intermediates Process for the preparation of norpatchoulenol and intermediates

1974-02-21

1978-11-07

Thomas, Jr., James O.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

C07C 2900

Patent

active

041246489

ABSTRACT:
A process for the preparation of norpatchoulenol is described according to the reaction scheme: ##STR1## Novel intermediates of formulae ##STR2## wherein R.sup.1 is methyl or benzyl and ##STR3## wherein R.sup.1 is methyl or benzyl and X is hydroxy, trityloxy, tosyloxy or halogen, are also described.

REFERENCES:
patent: 3673261 (1972-05-01), Kretschmar et al.
Buchli et al., "Constitution of Patchouli Alcohol and Absolute Configurat of Cedrene," J. Am. Chem. Soc., 83, 927-938 (1961).
Buchli, "Synthesis of Patchouli Alcohol," J. Am. Chem. Soc., 84, pp. 3205-3206 (1962).
Dobler et al., "The Structure of Patchouli Alcohol," Proc. Chem. Soc. (London), p. 383 (1963).
Buchli et al., "Synthesis of Patchouli Alcohol," J. Am. Chem. Soc. 86, pp. 4438-4444 (1964).
Hickinbottom, Reactions of Organic Compounds, pp. 138-143, (1957).
House, Modern Synthetic Reactions, pp. 11-12, (1972).
Reagents For Organic Synthesis, Fieser et al., (1967) pp. 46-47.

Affiliated with

Also associated with

Rating

Process for the preparation of norpatchoulenol and intermediates does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for the preparation of norpatchoulenol and intermediates, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for the preparation of norpatchoulenol and intermediates will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-2233649