Process for the preparation of N-sulfoalkyl quaternary salts of

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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548127, 548150, 548179, 548217, 548325, 548327, 548565, 260239R, C07D29312, C07D27762, C07D26354, C07D73504

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045046689

ABSTRACT:
Tertiary amines may be quaternized by heating them with a sulfoalkylating agent of this invention to a temperature of from 100.degree. to 250.degree. C. The sulfoalkylating agents which are believed to be hydroxy alkane sulfonic acid sulfoalkyl esters are free from sultone and are prepared by heating a hydroxy alkane sulfonic acid of propane or butane or the corresponding sultone to a temperature in the region of from 80.degree. to 180.degree. C. in the presence of water in an amount of 1 to 4 moles per mole of hydroxy alkane sulfonic acid or alkane sultone.

REFERENCES:
patent: 2912329 (1959-11-01), Jones et al.
patent: 4287348 (1981-09-01), Kitzing et al.
Maneche, Chem. Berichte, 85, pp. 160-163, (1952).

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