Process for the preparation of N,N'-tetrathiodimorpholine

Details Process for the preparation of N,N'-tetrathiodimorpholine Process for the preparation of N,N'-tetrathiodimorpholine

1986-09-04

1987-05-05

Ramsuer, Robert W.

Organic compounds -- part of the class 532-570 series

Organic compounds

Chalcogen in the nitrogen containing substituent

544110, C07D29522

Patent

active

046634550

ABSTRACT:
There is disclosed a process for the preparation of N,N'-tetrathiodimorpholine wherein an admixture of morpholine and elemental sulfur is oxidized with air or oxygen in the presence of iron salts or iron complexes in combination with zinc compounds such as ZnCl.sub.2 and ZnO to yield N,N'-tetrathiodimorpholine.

REFERENCES:
patent: 2351657 (1944-06-01), Bayes
patent: 2911405 (1959-11-01), Gregg, Jr.

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