Process for the preparation of methyl 3,4-anhydro-2,6-dideoxy-L-

Details Process for the preparation of methyl 3,4-anhydro-2,6-dideoxy-L- Process for the preparation of methyl 3,4-anhydro-2,6-dideoxy-L-

1977-11-14

1979-11-13

Brown, Johnnie R.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

536 1, 260343, 424180, 536 4, C07D30100

Patent

active

041743440

ABSTRACT:
A process to produce methyl 3,4-anhydro-2,6-dideoxy-L-ribohexopyranoside, its enantiomer and racemate thereof.
The compound is useful as an intermediate in the production of daunosamine which in turn is a prime constituent in the anti-cancer agents Daunomycin and Adriamycin. Also disclosed are novel intermediates in the process.

REFERENCES:
patent: 2916462 (1959-12-01), Koroch
patent: 3997663 (1976-12-01), Pennert et al.
Chem. Abstracts, 85, 62725d (1976).
Wong, C. M., et al., Con. J. Chem., 53,3144 (1975).
Cella, J. A., et al., J. Org. Chem., 42, 2077 (1977).
Corey, E. J. et al., Tetrahedron Lett., 311 (1970).
Richardson, A. C., Chem. Comm., 627 (1965).
March, J. P., et al., Chem. Comm., 973 (1967).
Horton, D. and Weckerle, W., Carboh Research, 44,227 (1975).
Partridge, J. J., et al., J. Amer. Chem. Soc., 95,532 (1973).

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