Organic compounds -- part of the class 532-570 series – Organic compounds – Azo
Patent
1990-06-08
1991-02-19
Higel, Floyd D.
Organic compounds -- part of the class 532-570 series
Organic compounds
Azo
534602, 534583, 534887, 534573, C09B 4100, C09B 4516, C09B 4520, C09B 6300
Patent
active
049945610
ABSTRACT:
A process for the preparation of an azo dye of formula ##STR1## wherein K is the .beta.-naphthol radical, X is hydrogen or nitro and M is an alkali metal ion or an ammonium ion, which process comprises coupling an aqueous solution containing 15 to 30 percent by weight of a diazo component of formula ##STR2## and 6 to 20 mol % of an ammonium salt, based on the molar amount of the diazo component, at a pH in the range from 10.5 to 11.5 and in an inert gas atmosphere, to a coupling component of formula ##STR3## in which formulae (2) and (3) above K and X are as defined for formula (1).
The present invention makes it possible to obtain the claimed azo dyes in high yield.
REFERENCES:
patent: 2812321 (1957-11-01), Eberhart et al.
Coloranti Azoici, Editura Technica Bucuresti (1981), 330-331.
Chem. Abstract 106:178104g (1987), Mitsui.
Huber Werner
Joswig Hans P.
Ciba-Geigy Corporation
Dohmann George R.
Higel Floyd D.
Mansfield Kevin T.
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