Process for the preparation of medium sized carbocyclic alkyl et

Details Process for the preparation of medium sized carbocyclic alkyl et Process for the preparation of medium sized carbocyclic alkyl et

1993-06-28

1995-05-09

Richter, Johann

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568659, C07C 4114

Patent

active

054141427

ABSTRACT:
An economically advantageous method is disclosed for the preparation without added solvent of a carbocyclic ether having from 10 to 16 carbon atoms in the ring of the formula ##STR1## wherein R is a straight or branched (C.sub.3 -C.sub.6) chain alkyl group or a benzyl group and n is from 5-11 carbon atoms, which method comprises: (1) reacting under an inert atmosphere a mixture consisting essentially of a carbocyclic alcohol of the formula ##STR2## wherein n is from 5-11 carbon atoms, about 1.5-10 molar equivalents of a straight or branch (C.sub.3 -C.sub.6) chain alkyl halide or benzyl halide and a metal hydride.

REFERENCES:
patent: 3876561 (1975-04-01), Naegeli
patent: 3993604 (1976-11-01), Thomas et al.
Streitwieser et al., Introduction to Organic Chemistry pp. 147-148 (1976).

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