Process for the preparation of lithium salts of anionic dyes by

Organic compounds -- part of the class 532-570 series – Organic compounds – Azo

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534583, 534617, 534622, 534626, 534627, 534629, 534632, 534633, 534635, 534636, 534637, 534638, 534642, 534887, 544355, 260371, 260372, C09B 4300, C09B 4600, C09B 6200, C09B 62503

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047075457

ABSTRACT:
Lithium salts of anionic dyes are prepared by first converting another salt of this anionic dye in aqueous solution or suspension by means of a compound which releases calcium ions into the water-insoluble or sparingly water-soluble calcium salt of the dye, which is separated from the aqueous medium and is then converted to an aqueous suspension by treatment with lithium sulfate or lithium hydrogensulfate or a mixture thereof in an equivalent amount of each or in an excess of up to 10% into its lithium salt.

REFERENCES:
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patent: 2796415 (1957-06-01), Ludwig et al.
patent: 3321457 (1967-05-01), Kissa
patent: 3600376 (1971-08-01), Franklin
patent: 3621008 (1971-11-01), Ross et al.
patent: 3635944 (1972-01-01), Litke
patent: 3655640 (1972-04-01), Hoare
patent: 4002603 (1977-01-01), Robbins et al.
Sisler et al, "General Chemistry, A Systematic Approach", The Macmillan Company, New York, pp. 214, 215 and 444 (1949).

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