Process for the preparation of lithium aluminum hydride in ether

Details Process for the preparation of lithium aluminum hydride in ether Process for the preparation of lithium aluminum hydride in ether

1996-02-12

1998-03-24

Langel, Wayne

Chemistry of inorganic compounds

Hydrogen or compound thereof

C01B 624

Patent

active

057309523

ABSTRACT:
A process for the preparation of lithium aluminum hydride in an ethereal solvent via the metathesis of sodium aluminum hydride and lithium chloride in a one direct step reaction comprising heating together sodium aluminum hydride and lithium chloride in an ethereal solvent at a temperature of 25.degree. C. to the reflux temperature of the solvent until the reaction is complete.

REFERENCES:
patent: 3162508 (1964-12-01), Bragdon et al.
patent: 3180700 (1965-04-01), Robinson
patent: 3207570 (1965-09-01), Noth
patent: 3337308 (1967-08-01), Verdieck et al.
patent: 3353930 (1967-11-01), Clasen et al.
patent: 3387947 (1968-06-01), Grendel
Direct Synthesis of Comlpex Metal Hydrides, E.C. Ashby, et al., Inorganic Chemistry, vol. 2, No. 3, Jun. 1963.

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