Process for the preparation of high absorptive sodium tripolypho

Compositions – Compositions containing a single chemical reactant or plural... – Organic reactant

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252 91, 252174, 423315, 427215, C01B 2541, C11D 3075, C11D 716, C11D 1102

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047342145

ABSTRACT:
Solid, free-flowing, essentially nonfriable powdery detergent particulates of recrystallized sodium tripolyphosphate hexahydrate having high absorption capacity and a pore volume of at least 0.70 cm.sup.3 /g, at lest 80% of the intercrystalline porosity thereof comprising pore sizes ranging from 0.5 .mu.m to 30 .mu.m, are prepared by (i) spraying water or an aqueous medium over a first fraction of anhydrous sodium tripolyphosphate, the majority of which fraction comprises phase 1 tripolyphosphate, (ii) spraying water or an aqueous medium over a separate second fraction of anhydrous sodium tripolyphosphate, which second fraction essentially consists of phase 2 triplyphosphate, (iii) intimately admixing said first and said second sprayed fractions, (iv) suspending the resulting admixture in water or an aqueous medium, and then (v) drying the resulting suspension, e.g., by atomization.

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patent: 4454054 (1984-06-01), Landgraber

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