Process for the preparation of halogenated alkanes

Details Process for the preparation of halogenated alkanes Process for the preparation of halogenated alkanes

1995-08-14

1999-05-11

Siegel, Alan

Organic compounds -- part of the class 532-570 series

Organic compounds

Halogen containing

570172, C07C17/30;21/18

Patent

active

059029145

ABSTRACT:
A process for the preparation of halogenated alkanes is provided. In particular, a process is provided for the highly selective preparation of haloalkanes, including 1,1,1,3,3-pentachloropropane, pentachlorobutane, and hepatchlorohexane, in good yield.

REFERENCES:
patent: 3862978 (1975-01-01), Decker et al.
Kotora et al. "Selective Addition of Polyhalogenated Compounds to Chlorosubstituted Ethenes Catalyzed by a Copper Complex," React. Kinet. Catal. Lett. vol. 44, No. 2, 415-419 (1991).
Bulletin of the Academy of Sciences of the USSR Division of Chem ICAL Science, vol. 29, No. 6, 1980.
Zhiryukina et al. Synthesis of Polychloroalkanes with Several Different Chlorine-Containing Groups, Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimcheskaya, No. 1, 152-157 (1983).
Kotora et al. "Addition of Tetrachloromethane to Halogenated Ethenes Catalyzed by Transition Metal Complexes," Journal of Molecular Catalysis, 77(1992) 51-60.

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