Process for the preparation of endo-6-hydroxybicyclo[2.2.1]hepta

Details Process for the preparation of endo-6-hydroxybicyclo[2.2.1]hepta Process for the preparation of endo-6-hydroxybicyclo[2.2.1]hepta

1977-12-14

1979-09-04

Morgenstern, Norma

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

2603433R, 562502, 568670, 568808, C07C 2900

Patent

active

041669150

ABSTRACT:
The title compound is prepared by contacting 6-oxatricyclo[3.2.1.1.sup.3,8 ]nonan-7-one with a stoichiometric amount of a reducing agent, such as lithium aluminum hydride, at reducing conditions, such as reflux temperature and pressure. This difunctional, endo-specific product is useful in the preparation of various polymer systems illustrated by polyesters, polyurethanes, polycarbonates, etc.

REFERENCES:
patent: 2778838 (1957-01-01), Abe et al.
patent: 2785184 (1957-03-01), Sanderson
patent: 2933506 (1960-04-01), Ohloff
Weygand et al. "Prep. Org. Chem", p. 79 (1972) John Wiley & Sons, New York.
Ramswami et al. "J. Org. Chem" 27:2761-2763 (1962).
Alder et al. "Justus Liebigs Ann der Chemies", vol. 514, pp. 197-211 (1934).

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