Process for the preparation of difructose dianhydride III

Details Process for the preparation of difructose dianhydride III Process for the preparation of difructose dianhydride III

1989-03-03

1991-10-15

Lilling, Herbert J.

Chemistry: molecular biology and microbiology

Micro-organism, tissue cell culture or enzyme using process...

Preparing compound containing saccharide radical

435 74, 435 97, 435100, 435101, 435105, 435193, 435830, C12P 1914, C12P 1912, C12R 106

Patent

active

050574183

ABSTRACT:
Disclosed herein is a process for preparing difructose dianhydride III (DFA III) comprising reacting inulin with an inulin lytic enzyme derived from a microorganism belonging to Arthrobacter ilicis. The enzyme employed herein efficiently produces DFA III from inulin and is more stable against heat than conventional enzymes. The present process enables industrial continuous production of DFA III. The preferred strain used herein is Arthrobacter ilicis MCI 2297 (FERM P-9893).

REFERENCES:
Biotech Derwent Abstract 89-03534, Kawamura et al., A BCHA6 Agric. Biol. Chem. (1985), 52, 12, 3209-3210.
J. Biochem., vol. 78, No. 6, 1975; "Enzymic Hydrolysis of Di-D-Fructofuranose 1, 2'; 2, 3' Dianhydride with Arthrobacter Ureafaciens", T. Tanaka, et al., pp. 1201-1206.
Carbohydrate Research, vol. 101, 1982; "Anomeric Configurations of Di-D-Fructose Anhydride III, Produced by Inulin D-Fructotransferase", T. Uchiyama et al., pp. 138-140.
Carbohydrate Research, vol. 107, 1982; "The Crystal Structure of Di-D-Fructose Anydride III, Produced by Inulin D-Fructotransferase", T. Taniguchi et al., pp. 255-262.
Agric. Biol. Chem., vol. 47, No. 2, 1983; "Formation of Di-D-Fructose Anhydrade III from Inulin by the Root of Lycoris Radiata Herbert", T. Uchiyama et al., pp. 437-439.
Agric. Biol. Chem., vol. 47, No. 12, 1983; "Effects of Some Substances on the Formation of Inulin Fructotransferase in Arthrobacter Ureafaciens", M. Nakayama, pp. 2761-2766.
Patent Abstracts of Japan, vol. 12, No. 165 (C-496), [3012], 18th May, 1988, p. 89, JP-A-62 275 694 (Natl. Food Res. Inst. (30-11-1987).
Agricultural and Biological Chemistry vol. 52, No. 12, Dec. 1988, pp. 3209-3210, The Agricultural Chemical Society of Japan; M. Kawamura et al., "Purification and Some Properties of Inulin Fructotransferase (Depolymerizing) from Arthobacter Ilicis".
Zentralblatt Bakteriol. Mikrobiol. Hyg. I. Abt. Orig., C2, 1981, pp. 318-323; M. D. Collins et al.: "Reclassification of Corynebacterium Ilicis (Mandel, Guba and Litsky) in the Genus Arthrobacter, as Arthrobactor Ilicis Comb. Nov.", p. 321, line 31, p. 322, line 17.

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