Process for the preparation of diazomethane

Details Process for the preparation of diazomethane Process for the preparation of diazomethane

2005-11-08

2005-11-08

Powers, Fiona T. (Department: 1626)

Organic compounds -- part of the class 532-570 series

Organic compounds

Diazo or diazonium

C534S558000

Reexamination Certificate

active

06962983

ABSTRACT:
A method for the production of diazomethane comprising the steps of a) feeding a base and a diazomethane precursor into a reactor vessel; b) generating gaseous diazomethane by allowing the base and the gaseous diazomethane precursor to react; and c) removing the gaseous diazomethane using a diluent gas.

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Proctor et al., “Development of a Continuous Process for the Industrial Generation of Diazomethane”, Organic Process Research and Development, 6, 884-892, 2002.
Bernd-Eistert, “Synthesis with Diazomethane”, 513-570, no date provided.
Black, T.H., “The Preparation and Reaction of Diazomethane,” Aldrichimica Acta 16(1) 3-10 (1983).
Chemistry in Industry, Feb. 21, 1994, p. 122/123, Nov. 5, 1990.
De Boer, T.H. J., and Backer, H. J., “A New Method for the Preparation of Diazomethane,” Recueil 73, 229-234 (1954).
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