Process for the preparation of cycloalkylalkane carboxylic acid

Details Process for the preparation of cycloalkylalkane carboxylic acid Process for the preparation of cycloalkylalkane carboxylic acid

1974-06-03

1976-01-20

Sutto, Anton H.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260514H, C07C 6138

Patent

active

039339033

ABSTRACT:
A process is disclosed for effectively producing a cycloalkylalkane carboxylic acid by reacting a cyclic ketone or a cyclic alcohol with a molten alkali metal hydroxide using a two step temperature treatment during the reaction wherein the first step temperature ranges from 200.degree. to 270.degree.C and the second step temperature ranges from 290.degree. to 350.degree.C. The alkali metal soap is then converted to the free acid. The process is especially directed to the manufacture of cyclopentylpropionic acid.

REFERENCES:
C & E. News, "Ketons Cleared at Room Temperature" Apr. 20, 1964.

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